TA Instruments

AR1768-0002f

28/03/2013 09:40:53

Sample name	DI 40 mm AL P80B 10 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	mr1
Sample density	1.000 g/cm^3
Results file name	AR1768
Run number	2 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	28/03/2013 09:40:53

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	40 mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	40.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	2.000 
Shear stress factor	79580 1/m^3
Measurement system factor	39790 1/m^3
Fluid density factor	8.378E-10 m^5
Normal force factor	1592 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	12.57 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	4.647	-150.75	10000	20.0	5.896	30.996	-12.00	9.295	-1.291	9384	2.0265	108.6	4.0530	405.30	3.411E-3	0.0	0.5
2.0120	10.11	13.789	10000	20.0	5.895	32.012	1.097	20.22	0.05427	9383	13.6637	22.95	27.327	2732.7	3.411E-3	0.0	0.5
2.9960	15.62	25.755	10000	20.0	5.894	32.996	2.050	31.23	0.06562	9380	27.3220	9.616	54.644	5464.4	3.411E-3	0.0	0.5
3.9960	18.53	33.531	10000	20.0	5.896	33.996	2.668	37.07	0.07198	9384	41.2067	6.829	82.413	8241.3	3.411E-3	0.1	0.6
4.9960	24.75	52.347	10000	20.0	5.892	34.996	4.166	49.50	0.08415	9377	67.8891	3.827	135.78	13578	3.411E-3	0.1	0.6
6.0200	31.64	78.437	10000	20.0	5.892	36.020	6.242	63.29	0.09862	9377	107.1450	2.341	214.29	21429	3.411E-3	0.1	0.6
6.9960	34.08	88.186	10000	20.0	5.892	36.996	7.018	68.16	0.1030	9378	126.6180	2.018	253.24	25324	3.411E-3	0.1	0.6
7.9960	39.35	111.24	10000	20.0	5.886	37.996	8.852	78.69	0.1125	9369	165.7350	1.513	331.47	33147	3.411E-3	0.1	0.6
9.0120	46.07	145.92	10000	20.0	5.880	39.012	11.61	92.14	0.1260	9358	223.4650	1.102	446.93	44693	3.411E-3	0.2	0.7
10.012	50.99	174.24	10000	20.0	5.873	40.012	13.87	102.0	0.1360	9347	275.0260	0.8988	550.05	55005	3.411E-3	0.2	0.7
11.016	55.75	202.74	10000	20.0	5.868	41.016	16.13	111.5	0.1447	9339	326.3790	0.7511	652.76	65276	3.411E-3	0.2	0.7
12.012	60.13	231.31	10000	20.0	5.860	42.012	18.41	120.3	0.1531	9327	377.5130	0.6450	755.03	75503	3.411E-3	0.2	0.7
13.012	64.43	261.36	10000	20.0	5.854	43.012	20.80	128.9	0.1614	9318	436.1800	0.5611	872.36	87236	3.411E-3	0.2	0.7
13.996	69.17	295.34	10000	20.0	5.845	43.996	23.50	138.3	0.1699	9303	499.2180	0.4862	998.44	99844	3.411E-3	0.2	0.7
14.996	75.69	351.25	10000	20.0	5.835	44.996	27.95	151.4	0.1846	9287	594.3530	0.4052	1188.7	1.1887E5	3.411E-3	0.2	0.7
15.996	79.94	387.16	10000	20.0	5.825	45.996	30.81	159.9	0.1927	9270	664.3880	0.3627	1328.8	1.3288E5	3.411E-3	0.3	0.8
16.996	84.54	429.80	10000	20.0	5.819	46.996	34.20	169.1	0.2023	9261	740.7850	0.3239	1481.6	1.4816E5	3.411E-3	0.3	0.8
18.012	90.99	494.33	10000	20.0	5.801	48.012	39.34	182.0	0.2162	9233	855.1740	0.2788	1710.3	1.7103E5	3.411E-3	0.3	0.8
19.012	95.05	532.90	10000	20.0	5.792	49.012	42.41	190.1	0.2231	9217	931.3700	0.2551	1862.7	1.8627E5	3.411E-3	0.3	0.8
20.012	99.41	584.63	10000	20.0	5.780	50.012	46.52	198.8	0.2340	9199	1020.2800	0.2327	2040.6	2.0406E5	3.412E-3	0.3	0.8
21.008	105.8	652.02	10000	20.0	5.758	51.008	51.89	211.7	0.2451	9165	1153.5800	0.2045	2307.2	2.3072E5	3.411E-3	0.4	0.9
22.012	109.9	702.62	10000	20.0	5.745	52.012	55.91	219.8	0.2544	9143	1242.8101	0.1892	2485.6	2.4856E5	3.411E-3	0.4	0.9
23.012	114.2	757.49	10000	20.0	5.735	53.012	60.28	228.5	0.2638	9128	1343.7500	0.1748	2687.5	2.6875E5	3.411E-3	0.4	0.9
24.016	120.7	833.75	10000	20.0	5.714	54.016	66.35	241.3	0.2750	9094	1496.3800	0.1562	2992.8	2.9928E5	3.411E-3	0.4	0.9
24.996	124.7	888.39	10000	20.0	5.693	54.996	70.70	249.5	0.2834	9060	1597.2500	0.1456	3194.5	3.1945E5	3.411E-3	0.4	0.9
25.996	129.1	942.18	10000	20.0	5.675	55.996	74.98	258.1	0.2905	9032	1711.1899	0.1356	3422.4	3.4224E5	3.411E-3	0.4	0.9
27.008	135.5	1035.9	10000	20.0	5.653	57.008	82.43	270.9	0.3043	8998	1882.0601	0.1226	3764.1	3.7641E5	3.411E-3	0.5	1.0
27.996	139.6	1096.7	10000	20.0	5.632	57.996	87.27	279.1	0.3126	8964	1996.0300	0.1150	3992.1	3.9921E5	3.411E-3	0.5	1.0
29.000	143.6	1158.1	10000	20.0	5.612	59.000	92.16	287.3	0.3208	8931	2116.1899	0.1082	4232.4	4.2324E5	3.411E-3	0.5	1.0
29.996	150.0	1265.5	10000	20.0	5.592	59.996	100.7	300.1	0.3356	8901	2305.9900	0.09884	4612.0	4.6120E5	3.411E-3	0.5	1.0
31.012	154.2	1328.2	10000	20.0	5.561	61.012	105.7	308.3	0.3428	8851	2432.6499	0.09310	4865.3	4.8653E5	3.411E-3	0.5	1.0
31.996	158.3	1393.0	10000	20.0	5.540	61.996	110.9	316.5	0.3502	8817	2566.8301	0.08801	5133.7	5.1337E5	3.411E-3	0.5	1.0
33.012	164.6	1513.8	10000	20.0	5.519	63.012	120.5	329.3	0.3658	8784	2775.5701	0.08101	5551.1	5.5511E5	3.411E-3	0.6	1.1
34.012	168.8	1575.2	10000	20.0	5.489	64.012	125.3	337.6	0.3713	8737	2913.6899	0.07666	5827.4	5.8274E5	3.411E-3	0.6	1.1
34.996	174.9	1691.6	10000	20.0	5.458	64.996	134.6	349.8	0.3849	8686	3127.5901	0.07100	6255.2	6.2552E5	3.411E-3	0.6	1.1
36.012	179.1	1767.3	10000	20.0	5.437	66.012	140.6	358.2	0.3926	8653	3279.1399	0.06742	6558.3	6.5583E5	3.411E-3	0.6	1.1
37.012	183.3	1857.6	10000	20.0	5.406	67.012	147.8	366.5	0.4033	8604	3430.8101	0.06404	6861.6	6.8616E5	3.411E-3	0.6	1.1
37.996	189.3	1962.5	10000	20.0	5.365	67.996	156.2	378.6	0.4125	8539	3659.5100	0.05958	7319.0	7.3190E5	3.411E-3	0.6	1.1
39.012	193.5	2046.6	10000	20.0	5.349	69.012	162.9	386.9	0.4209	8513	3822.2800	0.05686	7644.6	7.6446E5	3.411E-3	0.7	1.2
40.000	199.7	2162.3	10000	20.0	5.319	70.000	172.1	399.3	0.4309	8465	4068.4800	0.05308	8137.0	8.1370E5	3.411E-3	0.7	1.2
40.996	203.7	2241.1	10000	20.0	5.285	70.996	178.3	407.4	0.4378	8412	4232.6201	0.05069	8465.2	8.4652E5	3.411E-3	0.7	1.2
41.996	207.9	2353.7	10000	20.0	5.262	71.996	187.3	415.7	0.4505	8374	4409.5601	0.04845	8819.1	8.8191E5	3.411E-3	0.7	1.2
42.996	214.1	2480.0	10000	20.0	5.210	72.996	197.3	428.2	0.4609	8293	4676.4199	0.04523	9352.8	9.3528E5	3.411E-3	0.7	1.2
43.996	218.1	2571.1	10000	20.0	5.185	73.996	204.6	436.3	0.4690	8252	4851.2900	0.04336	9702.6	9.7026E5	3.411E-3	0.7	1.2
44.996	224.3	2698.8	10000	20.0	5.149	74.996	214.8	448.6	0.4787	8195	5128.8599	0.04072	10258	1.0258E6	3.411E-3	0.7	1.2
45.996	228.4	2794.3	10000	20.0	5.105	75.996	222.4	456.9	0.4867	8125	5318.2002	0.03893	10636	1.0636E6	3.411E-3	0.8	1.3
47.004	234.5	2944.0	10000	20.0	5.099	77.004	234.3	469.0	0.4995	8116	5602.2002	0.03689	11204	1.1204E6	3.411E-3	0.8	1.3
48.012	238.5	3046.2	10000	20.0	5.042	78.012	242.4	477.0	0.5081	8024	5797.7900	0.03526	11596	1.1596E6	3.411E-3	0.8	1.3
49.012	242.7	3124.6	10000	20.0	4.982	79.012	248.6	485.4	0.5123	7929	6001.7402	0.03366	12003	1.2003E6	3.411E-3	0.8	1.3
49.996	248.8	3286.0	10000	20.0	4.942	79.996	261.5	497.5	0.5256	7866	6303.2798	0.03178	12607	1.2607E6	3.411E-3	0.8	1.3
50.996	252.8	3389.2	10000	20.0	4.929	80.996	269.7	505.6	0.5334	7845	6510.5601	0.03069	13021	1.3021E6	3.411E-3	0.8	1.3
51.996	259.0	3521.9	10000	20.0	4.872	81.996	280.3	518.1	0.5410	7754	6833.2100	0.02889	13666	1.3666E6	3.411E-3	0.9	1.4
52.996	263.1	3627.0	10000	20.0	4.825	82.996	288.6	526.2	0.5485	7679	7046.5698	0.02773	14093	1.4093E6	3.411E-3	0.9	1.4
53.996	269.1	3815.9	10000	20.0	4.827	83.996	303.7	538.3	0.5641	7683	7374.4902	0.02651	14749	1.4749E6	3.411E-3	0.9	1.4
54.996	273.3	3913.6	10000	20.0	4.763	84.996	311.4	546.5	0.5698	7581	7602.8301	0.02538	15206	1.5206E6	3.411E-3	0.9	1.4
56.012	277.4	4025.6	10000	20.0	4.722	86.012	320.3	554.7	0.5775	7516	7828.6602	0.02443	15657	1.5657E6	3.411E-3	0.9	1.4
56.996	283.4	4205.6	10000	20.0	4.657	86.996	334.7	566.7	0.5905	7411	8184.6899	0.02308	16369	1.6369E6	3.411E-3	0.9	1.4
57.996	287.4	4309.4	10000	20.0	4.600	87.996	342.9	574.9	0.5965	7321	8408.4600	0.02215	16817	1.6817E6	3.411E-3	1.0	1.5
59.000	293.6	4471.5	10000	20.0	4.555	89.000	355.8	587.2	0.6060	7250	8767.7305	0.02103	17535	1.7535E6	3.411E-3	1.0	1.5
60.012	297.6	4592.7	10000	20.0	4.532	90.012	365.5	595.2	0.6141	7214	9009.7402	0.02036	18019	1.8019E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	300.0	4681.4	10000	20.0	4.472	91.000	372.5	600.0	0.6209	7117	308.8220	0.01977	617.64	61764	3.411E-3	0.0	1.5
1.9960	300.0	4684.1	10000	20.0	4.483	91.996	372.8	600.0	0.6213	7135	558.4840	0.01982	1117.0	1.1170E5	3.411E-3	0.0	1.5
2.9960	300.0	4684.1	10000	20.0	4.513	92.996	372.8	600.0	0.6213	7183	811.9060	0.01995	1623.8	1.6238E5	3.411E-3	0.0	1.5
3.9960	300.0	4657.1	10000	20.0	4.503	93.996	370.6	600.0	0.6177	7166	1186.9900	0.01991	2374.0	2.3740E5	3.411E-3	0.1	1.6
5.0000	300.0	4672.9	10000	20.0	4.516	95.000	371.9	600.0	0.6198	7188	1438.2200	0.01997	2876.4	2.8764E5	3.411E-3	0.1	1.6
6.0000	300.0	4681.7	10000	20.0	4.524	96.000	372.6	600.1	0.6209	7200	1815.1400	0.02000	3630.3	3.6303E5	3.411E-3	0.1	1.6
6.9960	300.0	4691.6	10000	20.0	4.488	96.996	373.3	600.0	0.6223	7143	2072.4399	0.01984	4144.9	4.1449E5	3.411E-3	0.1	1.6
7.9960	300.0	4694.9	10000	20.0	4.494	97.996	373.6	600.0	0.6227	7153	2317.9500	0.01987	4635.9	4.6359E5	3.411E-3	0.1	1.6
8.9920	300.0	4666.7	10000	20.0	4.479	98.992	371.4	600.0	0.6189	7129	2694.7300	0.01980	5389.5	5.3895E5	3.411E-3	0.1	1.6
9.9960	300.0	4669.9	10000	20.0	4.460	99.996	371.6	600.0	0.6194	7098	2947.3201	0.01972	5894.6	5.8946E5	3.411E-3	0.2	1.7
10.996	300.0	4680.2	10000	20.0	4.481	100.996	372.4	600.0	0.6207	7132	3325.5500	0.01981	6651.1	6.6511E5	3.411E-3	0.2	1.7
11.996	300.0	4674.5	10000	20.0	4.487	101.996	372.0	600.0	0.6200	7141	3574.5701	0.01984	7149.1	7.1491E5	3.411E-3	0.2	1.7
12.996	300.0	4654.0	10000	20.0	4.520	102.996	370.4	600.0	0.6172	7193	3825.8999	0.01998	7651.8	7.6518E5	3.411E-3	0.2	1.7
13.996	300.0	4686.3	10000	20.0	4.490	103.996	372.9	600.0	0.6215	7146	4204.9302	0.01985	8409.9	8.4099E5	3.411E-3	0.2	1.7
14.996	300.0	4700.9	10000	20.0	4.559	104.996	374.1	600.0	0.6235	7255	4455.3198	0.02015	8910.6	8.9106E5	3.411E-3	0.2	1.7
15.996	300.0	4659.4	10000	20.0	4.518	105.996	370.8	600.0	0.6179	7191	4706.7402	0.01997	9413.5	9.4135E5	3.411E-3	0.3	1.8
16.996	300.0	4673.9	10000	20.0	4.470	106.996	371.9	600.0	0.6199	7114	5082.6299	0.01976	10165	1.0165E6	3.411E-3	0.3	1.8
17.996	300.0	4691.9	10000	20.0	4.541	107.996	373.4	600.0	0.6223	7227	5333.6802	0.02007	10667	1.0667E6	3.411E-3	0.3	1.8
19.000	300.0	4675.5	10000	20.0	4.506	109.000	372.1	600.0	0.6202	7172	5713.4102	0.01992	11427	1.1427E6	3.411E-3	0.3	1.8
20.000	300.0	4686.3	10000	20.0	4.523	110.000	372.9	600.1	0.6215	7198	5961.9800	0.01999	11924	1.1924E6	3.411E-3	0.3	1.8
20.996	300.0	4688.6	10000	20.0	4.516	110.996	373.1	600.0	0.6219	7188	6215.3599	0.01997	12431	1.2431E6	3.411E-3	0.3	1.8
21.996	300.0	4670.9	10000	20.0	4.469	111.996	371.7	600.0	0.6195	7112	6591.6001	0.01976	13183	1.3183E6	3.411E-3	0.4	1.9
22.996	300.0	4689.0	10000	20.0	4.490	112.996	373.1	600.0	0.6219	7145	6844.1802	0.01985	13688	1.3688E6	3.411E-3	0.4	1.9
23.996	300.0	4641.9	10000	20.0	4.489	113.996	369.4	600.0	0.6156	7144	7220.9102	0.01984	14442	1.4442E6	3.411E-3	0.4	1.9
24.996	300.0	4670.7	10000	20.0	4.505	114.996	371.7	600.0	0.6195	7169	7469.9302	0.01991	14940	1.4940E6	3.411E-3	0.4	1.9
25.996	300.0	4645.6	10000	20.0	4.473	115.996	369.7	600.0	0.6161	7118	7721.4502	0.01977	15443	1.5443E6	3.411E-3	0.4	1.9
26.996	300.0	4657.7	10000	20.0	4.486	116.996	370.6	600.0	0.6177	7140	8098.3398	0.01983	16197	1.6197E6	3.411E-3	0.4	1.9
28.000	300.0	4658.0	10000	20.0	4.492	118.000	370.7	600.0	0.6178	7149	8349.8496	0.01985	16700	1.6700E6	3.411E-3	0.5	2.0
28.996	300.0	4695.6	10000	20.0	4.499	118.996	373.7	599.9	0.6228	7160	8600.9902	0.01989	17202	1.7202E6	3.411E-3	0.5	2.0
29.996	300.0	4678.1	10000	20.0	4.519	119.996	372.3	600.0	0.6205	7192	8979.4697	0.01998	17959	1.7959E6	3.411E-3	0.5	2.0
30.996	300.0	4649.9	10000	20.0	4.472	120.996	370.0	600.0	0.6167	7117	9229.2305	0.01977	18458	1.8458E6	3.411E-3	0.5	2.0
31.996	300.0	4677.7	10000	20.0	4.522	121.996	372.2	600.0	0.6204	7196	9606.3301	0.01999	19213	1.9213E6	3.411E-3	0.5	2.0
32.996	300.0	4679.6	10000	20.0	4.480	122.996	372.4	600.0	0.6207	7130	9857.7002	0.01980	19715	1.9715E6	3.411E-3	0.5	2.0
33.996	300.0	4689.5	10000	20.0	4.540	123.996	373.2	600.0	0.6219	7226	10113.900	0.02007	20228	2.0228E6	3.411E-3	0.6	2.1
34.996	300.0	4665.8	10000	20.0	4.489	124.996	371.3	600.0	0.6188	7144	10486.700	0.01984	20973	2.0973E6	3.411E-3	0.6	2.1
35.996	300.0	4668.1	10000	20.0	4.529	125.996	371.5	600.0	0.6191	7208	10737.300	0.02002	21475	2.1475E6	3.411E-3	0.6	2.1
37.000	300.0	4671.6	10000	20.0	4.512	127.000	371.8	600.0	0.6196	7182	11115.600	0.01995	22231	2.2231E6	3.411E-3	0.6	2.1
37.996	300.0	4650.4	10000	20.0	4.465	127.996	370.1	600.0	0.6168	7107	11365.700	0.01974	22731	2.2731E6	3.411E-3	0.6	2.1
38.996	300.0	4682.4	10000	20.0	4.476	128.996	372.6	600.0	0.6210	7123	11618.200	0.01979	23236	2.3236E6	3.411E-3	0.6	2.1
39.996	300.0	4665.6	10000	20.0	4.504	129.996	371.3	600.0	0.6188	7169	11994.100	0.01991	23988	2.3988E6	3.411E-3	0.7	2.2
40.996	300.0	4658.9	10000	20.0	4.467	130.996	370.7	600.0	0.6179	7109	12245.200	0.01975	24490	2.4490E6	3.411E-3	0.7	2.2
41.996	300.0	4679.6	10000	20.0	4.528	131.996	372.4	600.0	0.6207	7207	12624.900	0.02002	25250	2.5250E6	3.411E-3	0.7	2.2
42.996	300.0	4631.5	10000	20.0	4.487	132.996	368.6	600.1	0.6142	7142	12875.700	0.01983	25751	2.5751E6	3.411E-3	0.7	2.2
43.996	300.0	4672.3	10000	20.0	4.517	133.996	371.8	600.0	0.6197	7190	13126.100	0.01997	26252	2.6252E6	3.411E-3	0.7	2.2
44.996	300.0	4704.2	10000	20.0	4.524	134.996	374.4	600.0	0.6239	7201	13501.800	0.02000	27004	2.7004E6	3.411E-3	0.7	2.2
45.996	300.0	4648.7	10000	20.0	4.471	135.996	369.9	600.0	0.6166	7116	13753.200	0.01977	27506	2.7506E6	3.411E-3	0.8	2.3
46.996	300.0	4668.9	10000	20.0	4.514	136.996	371.5	600.0	0.6192	7184	14004.600	0.01996	28009	2.8009E6	3.411E-3	0.8	2.3
47.996	300.0	4656.6	10000	20.0	4.481	137.996	370.6	600.0	0.6176	7132	14381.600	0.01982	28763	2.8763E6	3.411E-3	0.8	2.3
48.992	300.0	4683.6	10000	20.0	4.477	138.992	372.7	600.0	0.6212	7126	14633.000	0.01979	29266	2.9266E6	3.411E-3	0.8	2.3
49.996	300.0	4689.9	10000	20.0	4.510	139.996	373.2	600.0	0.6220	7177	15012.200	0.01994	30024	3.0024E6	3.411E-3	0.8	2.3
50.996	300.0	4659.9	10000	20.0	4.514	140.996	370.8	600.0	0.6180	7184	15261.200	0.01995	30522	3.0522E6	3.411E-3	0.8	2.3
51.996	300.0	4695.6	10000	20.0	4.533	141.996	373.7	600.0	0.6228	7214	15512.700	0.02004	31025	3.1025E6	3.411E-3	0.9	2.4
53.000	300.0	4679.2	10000	20.0	4.501	143.000	372.4	600.0	0.6206	7163	15889.400	0.01990	31779	3.1779E6	3.411E-3	0.9	2.4
54.000	300.0	4676.3	10000	20.0	4.507	144.000	372.1	600.0	0.6202	7172	16140.800	0.01992	32282	3.2282E6	3.411E-3	0.9	2.4
55.000	300.0	4675.8	10000	20.0	4.539	145.000	372.1	600.0	0.6201	7225	16519.199	0.02007	33038	3.3038E6	3.411E-3	0.9	2.4
55.992	300.0	4696.9	10000	20.0	4.540	145.992	373.8	600.0	0.6229	7226	16770.400	0.02007	33541	3.3541E6	3.411E-3	0.9	2.4
56.996	300.0	4694.8	10000	20.0	4.514	146.996	373.6	600.0	0.6227	7183	17020.500	0.01995	34041	3.4041E6	3.411E-3	0.9	2.4
57.996	300.0	4649.9	10000	20.0	4.479	147.996	370.0	600.0	0.6167	7129	17398.600	0.01980	34797	3.4797E6	3.411E-3	1.0	2.5
58.996	300.0	4729.5	10000	20.0	4.585	148.996	376.4	600.0	0.6273	7297	17648.699	0.02027	35297	3.5297E6	3.411E-3	1.0	2.5
59.992	300.0	4736.2	10000	20.0	4.548	149.992	376.9	600.0	0.6281	7239	17902.500	0.02011	35805	3.5805E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	297.0	4562.9	10000	20.0	4.547	152.000	363.1	593.9	0.6114	7237	275.2340	0.02052	550.47	55047	3.411E-3	0.0	2.5
2.0160	293.0	4457.4	10000	20.0	4.573	153.016	354.7	585.9	0.6054	7277	513.1630	0.02120	1026.3	1.0263E5	3.411E-3	0.0	2.6
3.0360	286.8	4296.2	10000	20.0	4.608	154.036	341.9	573.7	0.5959	7334	870.2390	0.02228	1740.5	1.7405E5	3.411E-3	0.1	2.6
4.0160	282.7	4181.0	10000	20.0	4.677	155.016	332.7	565.4	0.5885	7444	1108.3500	0.02329	2216.7	2.2167E5	3.411E-3	0.1	2.6
5.0040	276.7	3985.9	10000	20.0	4.692	156.004	317.2	553.3	0.5732	7468	1446.2600	0.02439	2892.5	2.8925E5	3.411E-3	0.1	2.6
6.0200	272.6	3873.2	10000	20.0	4.716	157.020	308.2	545.2	0.5653	7506	1673.1500	0.02525	3346.3	3.3463E5	3.411E-3	0.1	2.6
7.0200	266.4	3720.2	10000	20.0	4.832	158.020	296.0	532.8	0.5556	7690	2011.4500	0.02709	4022.9	4.0229E5	3.411E-3	0.1	2.6
8.0000	262.4	3612.9	10000	20.0	4.854	159.000	287.5	524.8	0.5479	7726	2222.7000	0.02806	4445.4	4.4454E5	3.411E-3	0.1	2.7
8.9960	258.3	3528.2	10000	20.0	4.854	159.996	280.8	516.6	0.5435	7725	2435.4600	0.02895	4870.9	4.8709E5	3.411E-3	0.1	2.7
10.016	252.1	3370.6	10000	20.0	4.943	161.016	268.2	504.3	0.5319	7867	2754.6399	0.03094	5509.3	5.5093E5	3.411E-3	0.2	2.7
11.012	248.1	3273.9	10000	20.0	4.951	162.012	260.5	496.1	0.5251	7880	2955.0300	0.03201	5910.1	5.9101E5	3.411E-3	0.2	2.7
12.012	242.0	3142.3	10000	20.0	5.028	163.012	250.1	484.0	0.5166	8002	3258.3999	0.03416	6516.8	6.5168E5	3.411E-3	0.2	2.7
12.996	237.9	3008.7	10000	20.0	5.027	163.996	239.4	475.8	0.5032	8000	3455.6201	0.03534	6911.2	6.9112E5	3.411E-3	0.2	2.7
14.004	231.8	2861.7	10000	20.0	5.074	165.004	227.7	463.5	0.4913	8076	3745.3899	0.03759	7490.8	7.4908E5	3.411E-3	0.2	2.8
15.016	227.7	2773.9	10000	20.0	5.110	166.016	220.7	455.4	0.4847	8133	3931.2000	0.03922	7862.4	7.8624E5	3.411E-3	0.3	2.8
16.012	223.6	2684.1	10000	20.0	5.135	167.012	213.6	447.2	0.4777	8173	4119.8701	0.04087	8239.7	8.2397E5	3.411E-3	0.3	2.8
17.012	217.3	2530.0	10000	20.0	5.196	168.012	201.3	434.7	0.4632	8269	4395.5200	0.04376	8791.0	8.7910E5	3.411E-3	0.3	2.8
17.996	213.3	2465.4	10000	20.0	5.213	168.996	196.2	426.6	0.4599	8297	4569.3398	0.04559	9138.7	9.1387E5	3.411E-3	0.3	2.8
19.020	207.1	2339.2	10000	20.0	5.237	170.020	186.2	414.2	0.4494	8335	4832.9502	0.04857	9665.9	9.6659E5	3.411E-3	0.3	2.8
19.996	203.0	2243.1	10000	20.0	5.285	170.996	178.5	405.9	0.4397	8411	5000.8901	0.05105	10002	1.0002E6	3.411E-3	0.3	2.8
21.012	199.0	2160.4	10000	20.0	5.301	172.012	171.9	397.9	0.4320	8436	5163.4502	0.05328	10327	1.0327E6	3.411E-3	0.4	2.9
21.996	192.8	2024.4	10000	20.0	5.333	172.996	161.1	385.6	0.4178	8488	5407.3599	0.05709	10815	1.0815E6	3.411E-3	0.4	2.9
23.016	188.6	1944.0	10000	20.0	5.363	174.016	154.7	377.2	0.4102	8536	5570.0000	0.06001	11140	1.1140E6	3.411E-3	0.4	2.9
24.016	182.5	1831.2	10000	20.0	5.402	175.016	145.7	365.0	0.3993	8598	5797.5498	0.06454	11595	1.1595E6	3.411E-3	0.4	2.9
25.012	178.4	1744.6	10000	20.0	5.418	176.012	138.8	356.8	0.3891	8622	5947.6899	0.06774	11895	1.1895E6	3.411E-3	0.4	2.9
26.012	174.2	1686.9	10000	20.0	5.454	177.012	134.2	348.3	0.3854	8681	6095.4902	0.07155	12191	1.2191E6	3.411E-3	0.4	3.0
27.020	167.9	1567.0	10000	20.0	5.476	178.020	124.7	335.9	0.3713	8715	6307.9800	0.07726	12616	1.2616E6	3.411E-3	0.5	3.0
28.012	163.8	1499.7	10000	20.0	5.500	179.012	119.3	327.6	0.3643	8754	6444.8101	0.08156	12890	1.2890E6	3.411E-3	0.5	3.0
29.012	157.5	1426.1	10000	20.0	5.532	180.012	113.5	314.9	0.3604	8804	6651.9702	0.08878	13304	1.3304E6	3.411E-3	0.5	3.0
29.996	153.4	1311.3	10000	20.0	5.556	180.996	104.3	306.8	0.3401	8843	6775.7202	0.09395	13551	1.3551E6	3.411E-3	0.5	3.0
30.996	149.3	1249.4	10000	20.0	5.582	181.996	99.42	298.6	0.3329	8883	6900.5801	0.09962	13801	1.3801E6	3.411E-3	0.5	3.0
31.996	143.0	1151.8	10000	20.0	5.611	182.996	91.66	285.9	0.3206	8930	7088.8901	0.1092	14178	1.4178E6	3.411E-3	0.5	3.0
33.016	138.7	1092.9	10000	20.0	5.625	184.016	86.97	277.4	0.3136	8953	7206.2598	0.1164	14413	1.4413E6	3.411E-3	0.6	3.1
33.996	134.6	1021.2	10000	20.0	5.635	184.996	81.26	269.2	0.3018	8969	7318.5298	0.1237	14637	1.4637E6	3.411E-3	0.6	3.1
34.996	128.3	933.24	10000	20.0	5.661	185.996	74.27	256.5	0.2895	9011	7486.8799	0.1369	14974	1.4974E6	3.411E-3	0.6	3.1
36.016	124.0	866.64	10000	20.0	5.678	187.016	68.97	248.0	0.2781	9037	7593.8101	0.1469	15188	1.5188E6	3.411E-3	0.6	3.1
37.016	117.9	796.95	10000	20.0	5.709	188.016	63.42	235.7	0.2690	9086	7742.9702	0.1635	15486	1.5486E6	3.411E-3	0.6	3.1
38.000	113.6	740.38	10000	20.0	5.721	189.000	58.92	227.2	0.2593	9106	7842.0898	0.1764	15684	1.5684E6	3.411E-3	0.6	3.2
39.016	109.2	680.58	10000	20.0	5.737	190.016	54.16	218.3	0.2480	9130	7941.9600	0.1915	15884	1.5884E6	3.411E-3	0.7	3.2
39.996	105.0	638.71	10000	20.0	5.752	190.996	50.83	210.0	0.2420	9154	8028.8901	0.2076	16058	1.6058E6	3.411E-3	0.7	3.2
41.012	98.64	564.68	10000	20.0	5.770	192.012	44.94	197.3	0.2278	9184	8159.5601	0.2360	16319	1.6319E6	3.411E-3	0.7	3.2
42.012	94.18	513.46	10000	20.0	5.778	193.012	40.86	188.4	0.2169	9196	8246.5703	0.2592	16493	1.6493E6	3.411E-3	0.7	3.2
42.996	90.00	463.50	10000	20.0	5.794	193.996	36.88	180.0	0.2049	9221	8321.0996	0.2846	16642	1.6642E6	3.411E-3	0.7	3.2
43.996	83.62	406.75	10000	20.0	5.806	194.996	32.37	167.2	0.1935	9241	8433.5703	0.3304	16867	1.6867E6	3.411E-3	0.7	3.2
45.012	79.09	370.61	10000	20.0	5.813	196.012	29.49	158.2	0.1865	9251	8507.5596	0.3698	17015	1.7015E6	3.411E-3	0.8	3.3
45.992	74.90	330.00	10000	20.0	5.828	196.992	26.26	149.8	0.1753	9276	8569.5000	0.4133	17139	1.7139E6	3.411E-3	0.8	3.3
47.004	68.48	286.26	10000	20.0	5.841	198.004	22.78	137.0	0.1663	9296	8663.6299	0.4955	17327	1.7327E6	3.411E-3	0.8	3.3
47.996	63.85	249.66	10000	20.0	5.846	198.996	19.87	127.7	0.1556	9305	8724.6396	0.5706	17449	1.7449E6	3.411E-3	0.8	3.3
48.996	59.63	217.84	10000	20.0	5.851	199.996	17.33	119.3	0.1453	9312	8773.5400	0.6546	17547	1.7547E6	3.411E-3	0.8	3.3
49.996	55.38	189.39	10000	20.0	5.855	200.996	15.07	110.8	0.1361	9318	8823.3896	0.7597	17647	1.7647E6	3.411E-3	0.8	3.3
51.012	50.78	164.54	10000	20.0	5.861	202.012	13.09	101.6	0.1289	9328	8872.0996	0.9044	17744	1.7744E6	3.411E-3	0.9	3.4
52.012	44.05	129.41	10000	20.0	5.870	203.012	10.30	88.09	0.1169	9343	8933.5195	1.204	17867	1.7867E6	3.411E-3	0.9	3.4
53.000	39.69	107.91	10000	20.0	5.879	204.000	8.587	79.39	0.1082	9357	8970.2305	1.485	17940	1.7940E6	3.411E-3	0.9	3.4
54.012	34.83	84.626	10000	20.0	5.876	205.012	6.734	69.66	0.09668	9352	9006.7402	1.928	18013	1.8013E6	3.411E-3	0.9	3.4
55.012	29.73	64.285	10000	20.0	5.883	206.012	5.116	59.45	0.08604	9363	9036.9805	2.649	18074	1.8074E6	3.411E-3	0.9	3.4
56.012	25.36	49.234	10000	20.0	5.888	207.012	3.918	50.72	0.07724	9371	9061.1201	3.642	18122	1.8122E6	3.411E-3	0.9	3.5
57.012	20.16	33.353	10000	20.0	5.890	208.012	2.654	40.32	0.06583	9374	9084.7803	5.766	18170	1.8170E6	3.411E-3	1.0	3.5
58.000	14.36	18.213	10000	20.0	5.890	209.000	1.449	28.72	0.05046	9375	9102.1299	11.36	18204	1.8204E6	3.411E-3	1.0	3.5
59.016	9.582	8.5362	10000	20.0	5.894	210.016	0.6793	19.16	0.03544	9381	9113.4404	25.54	18227	1.8227E6	3.411E-3	1.0	3.5
59.996	6.219	3.1603	10000	20.0	5.893	210.996	0.2515	12.44	0.02022	9379	9118.2100	60.63	18236	1.8236E6	3.411E-3	1.0	3.5

